Webb Annual Reports on NMR Spectroscopy

1. Auflage 2011
ISBN: 978-0-12-391070-7
Verlag: Elsevier Science & Techn.
Format: EPUB
Kopierschutz: 6 - ePub Watermark

E-Book, Englisch, Band Volume 73, 234 Seiten

Reihe: Annual Reports on NMR Spectroscopy

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. - Provides updates on the latest developments in NMR spectroscopy - Includes comprehensive review articles - Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Autoren/Hrsg.

Webb, Graham A.

Inhaltsverzeichnis

1;Front Cover;1
2;Annual Reports on NMR Spectroscopy;4
3;Copyright Page;5
4;Contents;6
5;Contributors;8
6;Preface;10
7;Chapter 1: Recent Progress in the Solid-State NMR Studies of Biomineralization;12
7.1;1. Introduction;13
7.2;2. Methodology;14
7.3;3. NMR of Model Compounds;25
7.4;4. Model Systems of Biomineralization;44
7.5;5. Biominerals;55
7.6;6. Outlook;64
7.7;Acknowledgements;65
7.8;References;65
8;Chapter 2: Recent Advances in the NMR Spectroscopy of Chlorine, Bromine and Iodine;74
8.1;1. Introduction;75
8.2;2. Solid State NMR Spectroscopy;77
8.3;3. Solution Phase NMR Spectroscopy;83
8.4;4. Further Advances in Halogen NMR Spectroscopy;90
8.5;5. Concluding Comments;91
8.6;References;91
9;Chapter 3: Solution-State Dynamic Nuclear Polarization;94
9.1;1. Introduction;95
9.2;2. Theoretical Background;97
9.3;3. Experimental Results;107
9.4;4. Conclusion;131
9.5;References;131
10;Chapter 4: Solid-State NMR of Membrane Proteins: Moving Towards Greater Complexity;138
10.1;1. Introduction;139
10.2;2. Strategies for Overcoming Complexity and Focusing on Sites of Interest ;142
10.3;3. Solid-state NMR Snapshots of Membrane Proteins at Work;158
10.4;4. Conclusions;165
10.5;Acknowledgements;165
10.6;References;165
11;Chapter 5: Chromatographic NMR;170
11.1;1. Introduction;171
11.2;2. Methods to Achieve High-Resolution NMR Spectra in the Presence of Delaying Media;172
11.3;3. Mobility PFG;173
11.4;4. Examples of Chrom-NMR;177
11.5;5. Conclusions;182
11.6;Acknowledgements;183
11.7;References;183
12;Chapter 6: Kinetic Monte Carlo Simulation of DNMR Spectra;186
12.1;1. Introduction;187
12.2;2. Static NMR Spectra and the Description of Dynamic Exchange Processes;189
12.3;3. Calculation of DNMR Spectra with the Kinetic Monte Carlo Method;193
12.4;4. Summary;222
12.5;Acknowledgements;223
12.6;References;223
13;Subject Index;228