Webb Annual Reports on NMR Spectroscopy

1. Auflage 2010
ISBN: 978-0-12-381356-5
Verlag: Elsevier Science & Techn.
Format: EPUB
Kopierschutz: 6 - ePub Watermark

E-Book, Englisch, Band Volume 70, 246 Seiten

Reihe: Annual Reports on NMR Spectroscopy

In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. - Provides updates on the latest developments in NMR spectroscopy - Includes comprehensive review articles - Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Autoren/Hrsg.

Webb, Graham A.

Inhaltsverzeichnis

1;Front Cover;1
2;Annual Reports on NMR Spectroscopy;4
3;Copyright Page;5
4;Contents;6
5;Contributors;8
6;Preface;10
7;Chapter 1: Recent Developments in Liquid-State INADEQUATE Studies;12
7.1;1. Introduction;13
7.2;2. INADEQUATE-The Basic Concept;14
7.3;3. Increasing the Sensitivity of INADEQUATE;15
7.4;4. Measurement of 13C-13C Coupling Constants;25
7.5;5. Applications of High-Resolution INADEQUATE to 13C;30
7.6;6. Applications of INADEQUATE to Nuclei Other Than 13C;37
7.7;7. Outlook;43
7.8;References;43
8;Chapter 2: Phosphorus-31 NMR Spectroscopy of Condensed Matter;46
8.1;1. Introduction;47
8.2;2. Progress in Methodology;48
8.3;3. Applications of 31P SS NMR Spectroscopy;66
8.4;4. Concluding Remarks;118
8.5;Acknowledment;118
8.6;References;118
9;Chapter 3: Recent Applications of Solid-State 17O NMR;126
9.1;1. Introduction;127
9.2;2. 17O Synthesis;129
9.3;3. Background of Solid-State 17O NMR;131
9.4;4. Fundamentals of 17O NMR in Biological Solids;138
9.5;5. Applications of Solid-State 17O NMR in Biochemistry;159
9.6;6. Conclusions;166
9.7;References;167
10;Chapter 4: Spatial Inhomogeneity of Cavities in Polymer Network Systems as Characterised by Field-Gradient NMR Using Probe Diffusant Molecules andPolymers with Different Sizes ;170
10.1;1. Introduction;171
10.2;2. Network Structure of Polymer Gels and Diffusional Behaviour of Probe Polymers;172
10.3;3. Network Structure of Micrometre-Scale Cavity Obtained from Phase-Separated Polymer Blends as Characterised by Using Probe Molecules;203
10.4;4. Conclusions;210
10.5;References;210
11;Chapter 5: Practical NMR Analysis of Morphology and Structure of Polymers;214
11.1;1. Introduction;215
11.2;2. Analysis Method of Free Induction Decay of 1H Pulse NMR for Polymers;217
11.3;3. Morphology and Relaxation Behaviour;221
11.4;4. Kinetics of Dynamic Process of Polymers;240
11.5;5. Conclusions;249
11.6;References;249
12;Subject Index;252