Payling / Nelis Glow Discharge Optical Emission Spectroscopy

A Practical Guide
1. Auflage 2007
ISBN: 978-1-84755-098-9
Verlag: Royal Society of Chemistry
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, Band Volume 7, 224 Seiten

Reihe: RSC Analytical Spectroscopy Series

Glow discharge optical emission spectroscopy (GDOES) is an essential technique for the direct analysis of bulk solids, for elemental surface analysis and for the depth profiling of thin films and industrial coatings. The technique has shown rapid growth in numbers of instruments, in breadth of applications, in improved quantification in recent years and is now a recognised technique within the ISO, with two international standards. Glow Discharge Optical Emission Spectroscopy: A Practical Guide takes the reader on a journey through instrument operation, sample preparation, analysis, and reporting results. It follows two sets of samples through the whole process of analysis, brass samples for bulk analysis, and zinc-coated steel for depth profiling. Procedures are consistent with recent ISO standards and each step is loaded with hands-on tips and theoretical insight. The book also includes unique data tables on spectral interferences, molecular bands, self-absorption and relative sputtering rates. This book is designed for those using or managing GDOES instruments and for students interested in learning the technique from a hands-on perspective. It is also an invaluable aid to those considering the purchase of a GDOES instrument, or those using GDOES results, to understand in detail how the technique works and what is involved in maintaining the instrument and achieving high quality results.

Autoren/Hrsg.

Payling, Richard

Nelis, Thomas

Weitere Mitwirkende

Barnett, Neil W

Fachgebiete

• Naturwissenschaften Chemie Analytische Chemie Massenspektrometrie, Spektroskopie, Spektrochemie

Inhaltsverzeichnis

Preparation and Maintenance of Instrument;

Samples: Selection, Preparation;

Optimisation of Source and Analytical Parameters;

Calibration;

Calibration for Bulk Analysis;

Calibration for Compositional Depth Profiling;

Drift Correction;

Bulk Analysis;

Qualitative Depth Profiling;

Compositional Depth Profiling;

Theory;

Line Selection;

Trouble Shooting;

Subject Index