Naranjo C. / Noriega E. / Osswald Plastics Testing and Characterization

Industrial Applications
1. Auflage 2012
ISBN: 978-3-446-41853-0
Verlag: Carl Hanser
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 377 Seiten

Combined with a solid engineering background, this book provides the information and industrial case studies an engineer needs to both make informed decisions about selecting appropriate testing techniques and effectively troubleshoot problems in the field of plastics manufacturing.
The scope of this book also includes relevant and concise information for data interpretation using the most important characterization techniques.
Contents:

Spectroscopy
Gas Chromatography and Selective Mass Detection
Thermal Properties
Melt Rheology
Mechanical Properties
Permeability Properties
Environmental Effects and Aging
Electrical, Optical, and Acoustic Properties

Autoren/Hrsg.

Naranjo C., Alberto

Noriega E., María del Pilar

Noriega E., Maria del Pilar

Osswald, Tim A.

Roldán-Alzate, Alejandro

Sierra M., Juan Diego

Diego, Juan

Fachgebiete

• Technische Wissenschaften Maschinenbau | Werkstoffkunde Technische Mechanik | Werkstoffkunde Materialwissenschaft: Polymerwerkstoffe
• Technische Wissenschaften Verfahrenstechnik | Chemieingenieurwesen | Biotechnologie Technologie der Kunststoffe und Polymere

Inhaltsverzeichnis

1;PREFACE;8
2;TABLE OF CONTENTS;10
3;CHAPTER 1: INTRODUCTION;14
3.1;1.1 TESTING TECHNIQUES;14
3.2;1.2 STEPS FOR SUCCESSFUL POLYMER CHARACTERIZATION;17
3.3;1.3 PREPARATION AND SEPARATION TECHNIQUES;17
3.4;References;19
4;CHAPTER 2: SPECTROSCOPY;20
4.1;2.1 FTIR SPECTROSCOPY;21
4.1.1;2.1.1 FTIR Spectrophotometer;22
4.1.2;2.1.2 FTIR Techniques;24
4.1.3;2.1.3 Correlation of Polymer and Additives Structure and FTIR Spectra;27
4.1.4;2.1.4 Useful FTIR Standard Measuring Techniques;33
4.2;2.2 RAMAN SPECTROSCOPY;58
4.3;2.3 ENERGY DISPERSIVE X-RAY SPECTROSCOPY;64
4.4;References;66
5;CHAPTER 3: GAS CHROMATOGRAPHY AND SELECTIVE MASS DETECTION;68
5.1;3.1 GAS CHROMATOGRAPHY INSTRUMENTATION;68
5.2;3.2 CORRELATION OF ADDITIVE STRUCTURE AND MASS SPECTRA;72
5.3;3.3 SELECTED STANDARDS FOR GAS CHROMATOGRAPHY TESTING;75
5.4;References;86
6;CHAPTER 4: THERMAL PROPERTIES;88
6.1;4.1 THERMAL CONDUCTIVITY;88
6.2;4.2 SPECIFIC HEAT AND SPECIFIC ENTHALPY;93
6.3;4.3 DENSITY;97
6.4;4.4 THERMAL DIFFUSIVITY;97
6.4.1;4.4.1 New Developments in Thermal Diffusivity Measurement;101
6.5;4.5 LINEAR COEFFICIENT OF THERMAL EXPANSION;104
6.6;4.6 CURING BEHAVIOR;110
6.7;4.7 THERMAL ANALYSIS AND MEASURING DEVICES;113
6.7.1;4.7.1 Differential Scanning Calorimetry (DSC);115
6.7.2;4.7.2 Thermogravimetry (TGA);133
6.8;References;139
7;CHAPTER 5: MELT RHEOLOGY;140
7.1;5.1 BASIC CONCEPTS AND TERMINOLOGY;141
7.2;5.2 CONSTITUTIVE MODELS;155
7.2.1;5.2.1 Newtonian Model;156
7.2.2;5.2.2 Power Law Model;156
7.2.3;5.2.3 Bird-Carreau-Yasuda Model;157
7.2.4;5.2.4 Pressure Dependence of Viscosity;158
7.2.5;5.2.5 Phan-Thien and Tanner Multimode Model;159
7.3;5.3 RHEOMETRY;160
7.3.1;5.3.1 The Melt Flow Indexer;160
7.3.2;5.3.2 Capillary Viscometer;163
7.3.3;5.3.3 Rotational Rheometry;170
7.3.4;5.3.4 Extensional or Elongational Rheometry;178
7.4;References;196
8;CHAPTER 6: MECHANICAL PROPERTIES;198
8.1;6.1 MECHANICAL PROPERTIES;198
8.1.1;6.1.1 The Short-Term Tensile Test;198
8.1.2;6.1.2 Impact Strength;213
8.1.3;6.1.3 Creep Behavior;238
8.1.4;6.1.4 Dynamic Mechanical Tests;254
8.1.5;6.1.5 Fatigue Tests;259
8.1.6;6.1.6 Strength Stability Under Heat;266
8.2;References;273
9;CHAPTER 7: PERMEABILITY PROPERTIES;276
9.1;7.1 SORPTION;277
9.2;7.2 DIFFUSION AND PERMEATION;278
9.3;7.3 MEASURING S, D, AND P;288
9.4;7.4 DIFFUSION OF POLYMER MOLECULES AND SELF-DIFFUSION;294
9.5;References;298
10;CHAPTER 8: ENVIRONMENTAL EFFECTS AND AGING;300
10.1;8.1 WATER ABSORPTION;300
10.2;8.2 WEATHERING;304
10.3;8.3 CHEMICAL DEGRADATION;314
10.4;8.4 THERMAL DEGRADATION OF POLYMERS;321
10.5;References;327
11;CHAPTER 9: ELECTRICAL, OPTICAL, AND ACOUSTIC PROPERTIES;328
11.1;9.1 ELECTRICAL PROPERTIES;328
11.1.1;9.1.1 Dielectric Behavior;328
11.1.2;9.1.2 Electric Conductivity;334
11.1.3;9.1.3 Application Problems;339
11.1.4;9.1.4 Magnetic Properties;351
11.2;9.2 OPTICAL PROPERTIES;352
11.2.1;9.2.1 Index of Refraction;353
11.2.2;9.2.2 Photoelasticity and Birefringence;355
11.2.3;9.2.3 Transparency, Reflection, Absorption, and Transmittance;357
11.2.4;9.2.4 Gloss;362
11.2.5;9.2.5 Color;364
11.3;9.3 ACOUSTIC PROPERTIES;366
11.3.1;9.3.1 Speed of Sound;367
11.3.2;9.3.2 Sound Reflection;367
11.3.3;9.3.3 Sound Absorption;368
11.4;References;370
12;INDEX;372

Leseproben

Contents:

Spectroscopy
Gas Chromatography and Selective Mass Detection
Thermal Properties
Melt Rheology
Mechanical Properties
Permeability Properties
Environmental Effects and Aging
Electrical, Optical, and Acoustic Properties

Über Autor(innen)

Noriega E., María del Pilar
María del Pilar Noriega E., PhD, is R&D and Innovation Director at Daabon Group, Santa Marta, Colombia. Until 2019, she was the Director General of the ICIPC (Medellín, Colombia), and from 1997-2012 was Technical Director of the same institute.

Noriega E., Maria del Pilar
María del Pilar Noriega E., PhD, is R&D and Innovation Director at Daabon Group, Santa Marta, Colombia. Until 2019, she was the Director General of the ICIPC (Medellín, Colombia), and from 1997-2012 was Technical Director of the same institute.

Osswald, Tim A.
Tim A. Osswald, Ph.D., is Kuo and Cindy F. Wang Professor at the University of Wisconsin-Madison College of Engineering and Honorary Professor of Plastics Technology at the University of Erlangen-Nuremberg and the National University of Colombia. He is the author of many books and book chapters, as well as over 100 papers in the field of plastics technology.

María del Pilar Noriega E., PhD, is R&D and Innovation Director at Daabon Group, Santa Marta, Colombia. Until 2019, she was the Director General of the ICIPC (Medellín, Colombia), and from 1997-2012 was Technical Director of the same institute.
Tim A. Osswald, Ph.D., is Kuo and Cindy F. Wang Professor at the University of Wisconsin-Madison College of Engineering and Honorary Professor of Plastics Technology at the University of Erlangen-Nuremberg and the National University of Colombia. He is the author of many books and book chapters, as well as over 100 papers in the field of plastics technology.