Structure Elucidation by Modern NMR

A Workbook
3rd revidierte and updated ed
ISBN: 978-3-7985-1111-8
Verlag: Steinkopff

Buch, Englisch, 211 Seiten, Paperback, Format (B × H): 155 mm x 235 mm, Gewicht: 341 g

During the last few years, routine applications of NMR techniques have been further developed. Spectrometers of the latest generation offer new types of experiments, such as spinlock and inverse-detected methods. In this third, revised and expanded edition, new methodology is introduced and incorporated into new exercises. In addition, a new chapter has been introduced which demonstrates the fully detailed interpretation of two typical examples.

Zielgruppe

Professional/practitioner

Autoren/Hrsg.

Duddeck, Helmut

Toth, Gabor

Dietrich, Wolfgang

Inhaltsverzeichnis

Introduction.- Methodology.- High Magnetic Fields. One-dimensional 1H,1H Correlation. Two-Dimensional 1H,13C One-Bond Correlation. Two-Dimensional 1H,13C Long-Range Correlation. NOE Experiments. 13C,13C-Correlation.- Two Demonstration Examples. Rearrangement of a Benzothiazepine to a Benzothiazole Derivative. Structure Elucidation of a Triterpene Saponin.- Exercises.- Strategies.- Solutions.