X-Ray Diffraction

A Practical Approach
1998
ISBN: 978-0-306-45744-9
Verlag: Springer US

Buch, Englisch, 273 Seiten, Format (B × H): 160 mm x 241 mm, Gewicht: 1300 g

In this, the only book available to combine both theoretical and practical aspects of x-ray diffraction, the authors emphasize a "hands on" approach through experiments and examples based on actual laboratory data.
Part I presents the basics of x-ray diffraction and explains its use in obtaining structural and chemical information.
In Part II, eight experimental modules enable the students to gain an appreciation for what information can be obtained by x-ray diffraction and how to interpret it.
Examples from all classes of materials -- metals, ceramics, semiconductors, and polymers -- are included. Diffraction patterns and Bragg angles are provided for students without diffractometers. 192 illustrations.

Zielgruppe

Research

Autoren/Hrsg.

Norton, M. Grant

Suryanarayana, C.

Fachgebiete

• Technische Wissenschaften Verfahrenstechnik | Chemieingenieurwesen | Biotechnologie Metallurgie
• Technische Wissenschaften Maschinenbau | Werkstoffkunde Technische Mechanik | Werkstoffkunde Materialwissenschaft: Metallische Werkstoffe
• Technische Wissenschaften Maschinenbau | Werkstoffkunde Technische Mechanik | Werkstoffkunde Werkstoffkunde, Materialwissenschaft: Forschungsmethoden
• Naturwissenschaften Chemie Physikalische Chemie Chemische Kristallographie
• Geowissenschaften Geographie | Raumplanung Geographie: Allgemeines, Karten & Atlanten
• Technische Wissenschaften Sonstige Technologien | Angewandte Technik Bergbau, Hüttenwesen
• Technische Wissenschaften Maschinenbau | Werkstoffkunde Technische Mechanik | Werkstoffkunde Werkstoffprüfung

Inhaltsverzeichnis

I. Basics.- 1. X-Rays and Diffraction.- 2. Lattices and Crystal Structures.- 3. Practical Aspects of X-Ray Diffraction.- II. Experimental Modules.- Module 1. Crystal Structure Determination. I: Cubic Structures.- Module 2. Crystal Structure Determination. II: Hexagonal Structures.- Module 3. Precise Lattice Parameter Measurements.- Module 4. Phase Diagram Determination.- Module 5. Detection of Long-Range Ordering.- Module 6. Determination of Crystallite Size and Lattice Strain.- Module 7. Quantitative Analysis of Powder Mixtures.- Module 8. Identification of an Unknown Specimen.- Appendixes.- Appendix 1. Plane-Spacing Equations and Unit Cell Volumes.- Appendix 2. Quadratic Forms of Miller Indices for the Cubic System.- Appendix 3. Atomic and Ionic Scattering Factors of Some Selected Elements.- Appendix 4. Summary of Structure Factor Calculations.- Appendix 6. Multiplicity Factors.- Appendix 8. Physical Constants and Conversion Factors.- Appendix 9. JCPDS-ICDD Card Numbers for Some Common Materials.- Appendix 10. Crystal Structures and Lattice Parameters of Some Selected Materials.