Calibration in Analytical Science

Methods and Procedures
1. Auflage 2023
ISBN: 978-3-527-34846-6
Verlag: Wiley-VCH GmbH

Buch, Englisch, 384 Seiten, Format (B × H): 178 mm x 250 mm, Gewicht: 877 g

Calibration in Analytical Science

Designed to help analytical chemists save time and money by selecting the best calibration method in a quality control, substance monitoring, or research setting

Univariate analytical calibration is a vital step in every chemical procedure that involves determining the identity or concentration of a particular substance. Depending on the type of instrument and measurement, analytical chemists need to follow different calibration strategies and protocols to ensure their instruments yield accurate readings.

Calibration in Analytical Science systematically classifies and describes a wide range of calibration methods and procedures based on mathematical and empirical models for use in qualitative and quantitative analysis. Focusing on the chemical aspects of analytical calibration, this much-needed reference uses a set of equipment-independent terms and definitions that are easily transferable to the calibration strategies of any analytical process. The theoretical basis for calibration of each analytical mode is described and applied to common analytical tasks of increasing levels of difficulty and complexity. Throughout the book, the author illustrates how to combine different calibration approaches to create new calibration strategies with extended capabilities. - Describes different calibration methods and procedures for determining the nature and quantity of sample components in different ways
- Classifies various calibration methods in both qualitative and quantitative analysis

- Demonstrates how the random and systematic errors of an analytical method can be minimized by the proper calibration strategy

- Discusses current theoretical and methodological questions in calibration research
- Highlights how calibration approaches can diagnose, evaluate, and eliminate analytical errors

- Includes a concluding chapter on the contribution of calibration to the greening of analytical chemistry

Calibration in Analytical Science: Methods and Procedures is a must-have reference for analytical chemists working in academia and industry, chemists of various specialties involved in chemical analysis, and advanced undergraduate and graduate students taking courses in advanced analytical chemistry.

Autoren/Hrsg.

Koscielniak, Pawel

Ko´scielniak, Pawel

Fachgebiete

• Naturwissenschaften Chemie Analytische Chemie
• Naturwissenschaften Physik Physik Allgemein
• Technische Wissenschaften Verfahrenstechnik | Chemieingenieurwesen | Biotechnologie Pharmazeutische Technologie
• Naturwissenschaften Chemie Chemie Allgemein Pharmazeutische Chemie, Medizinische Chemie

Inhaltsverzeichnis

Introduction
PART I: Calibration in qualitative analysis
Calibrationless analysis
Theoretical calibration
Empirical calibration
Classification and error analysis
PART II: Calibration in quantitative analysis
Calibrationless analysis
Theoretical calibration
Empirical calibration
- Procedural classification
- Methodological classification
- Combined calibration methods
- Recovery in the calibration context
PART III: Calibration in semi-quantitative analysis
PART IV: Calibration in multivariate analysis
PART V: Calibration in the context of green analytical chemistry
Conclusion

Über Autor(innen)

Pawel Koscielniak received his Ph.D. in Chemistry in 1981 from the Jagiellonian University in Krakow, where he is now a full professor (since 2000) and heads the Department of Analytical Chemistry. He is a member of the Committee of Analytical Chemistry of the Polish Academy of Sciences. Prof. Koscielniak is the author, co-author and editor of more than 300 scientific articles, books and book chapters. The main areas of his scientific interest are flow analysis, forensic chemistry and environmental analysis with special attention paid to such issues as analytical calibration, examination and elimination of interference effects, optimization and validation of analytical procedures.